Ph2S/selectfluor-promoted deoxydifluorination of aldehydes

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成果类型：

期刊论文

作者：

He, Guowen;Xiao, Xuan;Jin, Han-Zhou;Lin, Jin-Hong*;Zhong, Tongsheng*;...

通讯作者：

Lin, Jin-Hong;Zhong, Tongsheng;Xiao, Ji-Chang;Zheng, Xing

作者机构：

[Lin, JH; Zhong, TS; Zhong, Tongsheng; Lin, Jin-Hong; He, Guowen] Hunan City Univ, Coll Mat & Chem Engn, Yiyang 413000, Peoples R China.

[Xiao, Xuan; Jin, Han-Zhou; Lin, Jin-Hong; Xiao, Ji-Chang; Lin, JH] Univ Chinese Acad Sci, Chinese Acad Sci, Shanghai Inst Organ Chem, Key Lab Organofluorine Chem, Beijing, Peoples R China.

[Xiao, Xuan; Zheng, Xing] Univ South China, Hunan Prov Cooperat Innovat Ctr Mol Target New Dr, Grp Lead Compound,Dept Pharm, Hunan Prov Key Lab Tumor Microenvironm Respons Dr, Hengyang 421001, Hunan, Peoples R China.

通讯机构：

[Lin, JH; Zhong, TS] H

[Lin, JH; Xiao, JC; Zheng, Xing] U

Hunan City Univ, Coll Mat & Chem Engn, Yiyang 413000, Peoples R China.

Univ Chinese Acad Sci, Chinese Acad Sci, Shanghai Inst Organ Chem, Key Lab Organofluorine Chem, Beijing, Peoples R China.

Univ South China, Hunan Prov Cooperat Innovat Ctr Mol Target New Dr, Grp Lead Compound,Dept Pharm, Hunan Prov Key Lab Tumor Microenvironm Respons Dr, Hengyang 421001, Hunan, Peoples R China.

语种：

英文

关键词：

Deoxydifluorination;Aldehydes;Difluoromethyl;Sulfur fluorine

期刊：

Tetrahedron

ISSN：

0040-4020

年：

2021

卷：

页码：

131963

DOI：

10.1016/j.tet.2021.131963

基金类别：

National Natural Science FoundationNational Natural Science Foundation of China (NSFC) [21971252, 21991122]; Key Research Program of Frontier Sciences, Chinese Academy of Sciences (CAS) [QYZDJSSWSLH049]; Youth Innovation Promotion Association CAS [2019256]; Science and Technology Department of Gansu Province [19ZD2GC001]; Key Project Foundation of Hunan Provincial Education Department [19A085]; Natural Science Foundation of Hunan ProvinceNatural Science Foundation of Hunan Province [2017JJ2018]

机构署名：

本校为第一且通讯机构

院系归属：

材料与化学工程学院

摘要：

The installation of a HCF2 group is a research area that has received increasing attention, and deoxydifluorination of aldehydes have served as an attractive protocol due to the wide availability of aldehydes. Herein we describe a Ph2S/Selectfluor-promoted deoxydifluorination of aldehydes under mild conditions. Compared with previous deoxydifluorination methods, which usually use hazardous reagents such as SF4, DAST and Deoxo-Fluor, this protocol is quite attractive because of the safe and convenient operations, and the use of ...

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