A new type of iron-carbon micro-electrolysis material is prepared by the roasting method,with iron powder, activated carbon and copper oxide as raw materials,bentonite as binder and a small amount of additives. Then it is used to treat Cr(Ⅵ) in aqueous solution. The results show that when the mass ratio of iron to carbon is 2∶1,the mass ratio of iron to copper oxide is 6∶1,the mass fraction of bentonite is 20%,the mass fraction of ammonium carbonate is 0.5%,the roasting temperature is 400 ℃,and the roasting time is 1.0 h,the prepared iron-c...