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Highly chemoselective synthesis of 1,2,3,4,5-pentasubstituted cyclohexanols under solvent-free condition

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成果类型:
期刊论文
作者:
Luo, Xinxiang;Shan, Zixing*
通讯作者:
Shan, Zixing
作者机构:
[Shan, Zixing] Wuhan Univ, Dept Chem, Wuhan 430072, Peoples R China.
Hunan City Univ, Dept Environm Chem & Engn, Yayang 413049, Hunan, Peoples R China.
通讯机构:
[Shan, Zixing] W
Wuhan Univ, Dept Chem, Wuhan 430072, Peoples R China.
语种:
英文
关键词:
MICHAEL REACTION;TRIKETONE;PYRIDINES;ALDOL
期刊:
Tetrahedron Letters
ISSN:
0040-4039
年:
2006
卷:
47
期:
32
页码:
5623-5627
机构署名:
本校为其他机构
院系归属:
材料与化学工程学院
摘要:
Acetophenone reacted with a series of aromatic aldehydes with grinding under catalysis of a double-component solid base system consisting of NaOH and K2CO3 to furnish highly chemoselectively 1,2,3,4,5-pentasubstituted cyclohexanols in 80-95% yield, and their composition and structure are identified by spectral technologies and single crystal X-ray diffraction analysis, and a possible mechanism of the formation was sugg...

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