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Preparation and characterization of poly(amic acid)-stabilized silver nanoparticles

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成果类型:
期刊论文
作者:
Li Jun;Fang Yue-cheng;He Guo-wen;Li Heng-feng*
通讯作者:
Li Heng-feng
作者机构:
[Fang Yue-cheng; He Guo-wen; Li Heng-feng; Li Jun] Cent South Univ, Sch Mat Sci & Engn, Changsha 410083, Hunan, Peoples R China.
[He Guo-wen] Hunan City Univ, Coll Chem & Environm Engn, Yiyang 413000, Peoples R China.
通讯机构:
[Li Heng-feng] C
Cent South Univ, Sch Mat Sci & Engn, Changsha 410083, Hunan, Peoples R China.
语种:
英文
关键词:
Diffusion controlled growth;Heterogeneous nucleation;Poly(amic acid);Polycrystalline state;Reaction mixture;Reduction of silver nitrates;Silver nanoparticles;Spherical morphologies;Crystallization kinetics;Nanoparticles;Nitrogen compounds;Ultraviolet visible spectroscopy;Silver
关键词(中文):
银纳米颗粒;聚酰胺酸;稳定剂;Avrami方程;银纳米粒子;表征;制备;表面等离子体
期刊:
中南大学学报(英文版)
ISSN:
2095-2899
年:
2013
卷:
20
期:
6
页码:
1475-1481
基金类别:
Foundation item: Project(10JJ5057) supported by the Hunan Provincial Natural Science Foundation of China Received date: 2012−03−09; Accepted date: 2012−07−20 Corresponding author: LI Heng-feng, Professor, PhD; Tel: +86−731−88877873; E-mail: lihengfeng@gmail-com-s.stat.lib.xjtu.edu.cn:443
机构署名:
本校为其他机构
院系归属:
材料与化学工程学院
摘要:
Stable and monodispersed silver nanoparticles were produced through a mild, convenient, one-pot method based on the reduction of silver nitrate in the presence of poly(amic acid) (PAA) as a stabilizer. The surface plasma band transition was monitored along with time in the reaction mixture for three sets of experiments by ultraviolet-visible spectroscopy. Analysis of the data with the Avrami equation yielded n exponent with values between 0.5 and 1.5, demonstrating three-dimensional heterogeneous nucleation and diffusion-controlled growth, acco...

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