Diclofenac (DCF), as a typical representative of PPCPs, has potential ecotoxicity to the water environment. In this study, ultrasound (US) enhanced ferrous sulfide (FeS)-activated persulfate (PDS) technology (US/FeS/PDS) was used to degrade DCF. By comparing the degradation effects of US, US/PDS, FeS/PDS and US/FeS/PDS systems on DCF, this study confirmed the synergy and strengthening effects of US. The influences of single-factor experimental conditions on the US/FeS/PDS system were investigated and optimized. The FeS catalysts before and afte...